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The Cr—N bipy bond lengths are in the range 2. As a prerequisite for possible applications, a detailed study of the structural and spectroscopic properties is needed.
The Cr—N bipy bond lengths are in the range of 2.
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The latter is chro,ium to the values of 1. The Cr—Cl bond length in Ihowever, is slightly shorter than those with 2. A search of the Cambridge Structural Database Version 5. All chemicals were reagent grade materials and used without further purification. The starting material, cis -[CrF 2 bipy 2 ]ClO 4 was prepared according to the literature Glerup et al. The crude perchlorate 0.
The filtrate was slowly evaporated at room temperature to yield orange crystals of I suitable for X-ray structural analysis. Table 2 Experimental details. In the crystal, the molecules are stacked along tesis a axis. The solution mixture was refluxed for 30 min and filtered. Crystal data, data collection and structure refinement chromiym are summarized in Table 2.
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An approximate isotropic treatment of cell e. E 66m—m Acta, — Acta Part A68— E 64m E 67m Acta Part A65— Methods in EnzymologyVol. PhD thesis, University of Basel, Switzerland.
thesi A 713—8. C 713—8. Acta64L85—L E 63m—m This is an open-access article distributed under the terms of the Creative Commons Attribution CC-BY Licencewhich permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
Download PDF of article. Synthesis and crystallization 6. Refinement Supporting information References. Figure 2 The crystal packing in Iviewed perpendicular to the bc plane. Synthesis and crystallization All chemicals were reagent grade materials and used without further purification. Supporting information CCDC reference: Synthesis and crystallization top.
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Refinement top Refinement on F 2 3 restraints Least-squares matrix: Special details top Geometry. The IUCr is a scientific union serving the interests of crystallographers and other scientists employing crystallographic methods.
Crystal system, space group. H atoms treated by a mixture thesiss independent and constrained refinement. The structure of the molecular components in Ishowing the atom-numbering scheme. The crystal packing in Iviewed perpendicular to the bc plane.